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Mar Drugs
2012 Jul 01;107:1498-1510. doi: 10.3390/md10071498.
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Further insights on the carotenoid profile of the echinoderm Marthasterias glacialis L.
Mariutti LRB
,
Pereira DM
,
Mercadante AZ
,
Valentão P
,
Teixeira N
,
Andrade PB
.
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In this study, the carotenoid profile of the echinoderm Marthasterias glacialis L. was established using HPLC-DAD-APCI-MS/MS equipped with a C(30) column. This approach rendered the identification of 20 compounds, eight of them reported for the first time in this marine organism. Differentiation of carotenoid isomers was also achieved.
Figure 1. Chromatogram (processed at 450 nm), obtained by HPLC-DAD, of the carotenoids from Marthasterias glacialis. See text for chromatographic conditions. Peak identification and characterization are given in Table 1.
Figure 2. Chromatogram (processed at 450 nm), obtained by HPLC-DAD, of astaxanthin standard submitted to heat under reflux. See text for chromatographic conditions. Peak identification and characterization are given in Table 2.
Figure 3. Chromatogram (processed at 450 nm), obtained by HPLC-DAD, of astaxanthin standard submitted to reduction with NaBH4. See text for chromatographic conditions. Peak identification and characterization are given in Table 3.
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